2-METHYL-DL-TYROSINE synthesis

3synthesis methods

Product Name:2-METHYL-DL-TYROSINE
CAS Number:96646-27-4
Molecular formula:C10H13NO3
Molecular Weight:195.22

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: NBS / CCl₄ / 1 h / Irradiation
2: NaH / dimethylformamide / 1 h
3: 1) 48percent HBr, 2) propylene oxide / 1) reflux, 6h, 2) i-PrOH, room temperature

References:

McDonald, Ian A.;Nyce, Philip L.;Jung, Michel J.;Sabol, Jeffrey S. [Tetrahedron Letters,1991,vol. 32,# 7,p. 887 - 890]

1-Bromomethyl-4-methoxy-2-methyl-benzene

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References

Propanedioic acid, 2-(acetylamino)-2-[(4-methoxy-2-methylphenyl)methyl]-, 1,3-diethyl ester

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References

2-METHYL-DL-TYROSINE Related Search:

BOC-7-HYDROXY-D-TIC-OH L-TYROSINE, N[(1,1-DIMETHYLETHOXY) CARBONYL] -2,6 7-HYDROXY-1,2,3,4-TETRAHYDROISOQUINOLINE-3-CARBOXYLIC ACID