2-((MethylaMino)Methyl)phenylboronic acid synthesis
- Product Name:2-((MethylaMino)Methyl)phenylboronic acid
- CAS Number:365245-83-6
- Molecular formula:C8H12BNO2
- Molecular Weight:165
Yield:365245-83-6 91%
Reaction Conditions:
Stage #1: 2-formylbenzene boronic acid;methylaminewith 4 A molecular sieve in methanol at 0 - 20; for 3.5 h;
Stage #2: with sodium tetrahydridoborate in methanol at 20; for 1 h;
References:
Swamy;Jang, Yun Jung;Park, Min Sun;Koh, Hwa Soo;Lee, Sang Kil;Yoon, Yeo Joon;Yoon, Juyoung [Tetrahedron Letters,2005,vol. 46,# 20,p. 3453 - 3456]
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