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ChemicalBook CAS DataBase List 2-Methylene-1,3-dioxepane

2-Methylene-1,3-dioxepane synthesis

8synthesis methods
-

Yield:69814-56-8 97.4%

Steps:

14 EXAMPLE 14

EXAMPLE 14 The procedure was as in Example 12, except that 32.0 g (0.25 mol) of 2,6-dimethylcyclohexanol were used instead of the 3,3-dimethylbutan-2-ol. The conversion of 2-chloromethyl-1,3-dioxepane was 97.4% and the yield of 2-methylene-1,3-dioxepane was 87.9%.

References:

US5455361,1995,A

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