![](/CAS/GIF/69814-56-8.gif)
2-Methylene-1,3-dioxepane synthesis
- Product Name:2-Methylene-1,3-dioxepane
- CAS Number:69814-56-8
- Molecular formula:C6H10O2
- Molecular Weight:114.14
![1,3-Dioxepane, 2-(chloromethyl)-](/CAS/20200515/GIF/54237-96-6.gif)
54237-96-6
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![2,6-DIMETHYLCYCLOHEXANOL](/CAS/GIF/5337-72-4.gif)
5337-72-4
50 suppliers
$44.00/25mL
![2-Methylene-1,3-dioxepane](/CAS/GIF/69814-56-8.gif)
69814-56-8
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$70.00/100mg
Yield:69814-56-8 97.4%
Steps:
14 EXAMPLE 14
EXAMPLE 14 The procedure was as in Example 12, except that 32.0 g (0.25 mol) of 2,6-dimethylcyclohexanol were used instead of the 3,3-dimethylbutan-2-ol. The conversion of 2-chloromethyl-1,3-dioxepane was 97.4% and the yield of 2-methylene-1,3-dioxepane was 87.9%.
References:
US5455361,1995,A
![2-BROMOMETHYL-[1,3]DIOXEPANE](/StructureFile/ChemBookStructure3/GIF/CB4290553.gif)
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![2-Methylene-1,3-dioxepane](/CAS/GIF/69814-56-8.gif)
69814-56-8
73 suppliers
$70.00/100mg
![1,3-Dioxepane, 2-(chloromethyl)-](/CAS/20200515/GIF/54237-96-6.gif)
54237-96-6
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![2-Methylene-1,3-dioxepane](/CAS/GIF/69814-56-8.gif)
69814-56-8
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$70.00/100mg
![2-Methyl-2-butanol](/CAS/GIF/75-85-4.gif)
75-85-4
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$9.00/10ml
![1,3-Dioxepane, 2-(chloromethyl)-](/CAS/20200515/GIF/54237-96-6.gif)
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![tert-Butyl methyl ether](/CAS/GIF/1634-04-4.gif)
1634-04-4
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$14.00/100g
![Ethylene glycol](/CAS/GIF/107-21-1.gif)
107-21-1
1316 suppliers
$10.00/25g
![2-Methylene-1,3-dioxepane](/CAS/GIF/69814-56-8.gif)
69814-56-8
73 suppliers
$70.00/100mg