2-(METHYLSULFONYL)-1-PYRIDIN-3-YLETHANONE synthesis

1synthesis methods

Product Name:2-(METHYLSULFONYL)-1-PYRIDIN-3-YLETHANONE
CAS Number:27302-95-0
Molecular formula:C8H9NO3S
Molecular Weight:199.23

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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124-63-0
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$10.00/5g

2-(METHYLSULFONYL)-1-PYRIDIN-3-YLETHANONE

27302-95-0
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$44.00/1g

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Yield: 80% ， 4.5%

Reaction Conditions:

with triethylamine in dichloromethane1.) ice cooling, 1 h; 2.) R_.T_., 2 h; than overnight.;

References:

Koikov, L. N.;Terent'ev, P. B.;Gloriozov, I. P.;Torocheshnikov, V. N.;Baidin, V. N.;Bundel', Yu. G. [Chemistry of Heterocyclic Compounds,1983,vol. 19,# 5,p. 518 - 524][Khimiya Geterotsiklicheskikh Soedinenii,1983,vol. 19,# 5,p. 643 - 650]