2-MORPHOLIN-4-YLACETOHYDRAZIDE synthesis
- Product Name:2-MORPHOLIN-4-YLACETOHYDRAZIDE
- CAS Number:770-17-2
- Molecular formula:C6H13N3O2
- Molecular Weight:159.19
35855-10-8
53 suppliers
$48.70/5g
770-17-2
36 suppliers
$22.00/250mg
Yield:770-17-2 95%
Reaction Conditions:
with hydrazine in ethanol at 90; for 18 h;
Steps:
85.A Synthesis of 3-(6-Methoxynaphthalen-2-yl)-5-(5-Morpholin-4-Ylmethyl-1H-[1,2,4]Triazol-3-yl)-1H-Indazole (CC001)
A. Morpholin-4-yl-acetic acid hydrazide A solution of methyl morpholinoacetate (2.43 g, 15.3 mmol), ethanol (20 mL) and hydrazine (0.53 mL, 16.8 mmol) was stirred at 90° C. for 18 hours. The mixture was concentrated and dried to provide the title compound (2.30 g, 95%): ES-MS (m/z) 160 [M+1]+
References:
US2005/107386,2005,A1 Location in patent:Page/Page column 46
3235-82-3
88 suppliers
$6.00/1g
770-17-2
36 suppliers
$22.00/250mg