2-N-CBZ-AMINO-CYCLOHEXANONE synthesis

7synthesis methods

Product Name:2-N-CBZ-AMINO-CYCLOHEXANONE
CAS Number:31236-61-0
Molecular formula:C14H17NO3
Molecular Weight:247.29

92645-06-2
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$446.00/5g

31236-61-0
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$500.10/5MG

Yield:31236-61-0 3.3 g

Reaction Conditions:

with Jones reagent at 20; for 2.5 h;

Steps:

93 Preparation 93: Benzyl (2-oxocyclohexyl)carbamate

Preparation 93: Benzyl (2-oxocyclohexyl)carbamate [0423] liquid (3.3 g). ¹H NMR (300 MHz, CDCl₃) δ 7.36-7.29 (m, 5H), 5.75 (br s, 1H), 5.10 (s, 2H), 4.29-4.25 (m, 1H), 2.65 (m, 1H), 2.57-2.50 (m, 1H), 2.43-2.33 (m, 1H), 2.17-2.10 (m, 1H), 1.88-1.60 (m, 3H), 1.48-1.34 (m, 1H). ESI (m/z): 248.0 (M+H).

References:

US2013/303524,2013,A1 Location in patent:Paragraph 0423-0424

6850-38-0 Synthesis