2-Nitro-1-naphthol synthesis
- Product Name:2-Nitro-1-naphthol
- CAS Number:607-24-9
- Molecular formula:C10H7NO3
- Molecular Weight:189.17
132-53-6
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$61.00/5g
607-24-9
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$9.00/1g
Yield:607-24-9 90.1%
Reaction Conditions:
with ethanol;lithium hydroxide monohydrate;dihydrogen peroxide;sodium hydroxide at 70; for 0.583333 h;Temperature;
Steps:
1.2; 2.2; 3.2 (2) Synthesis of 2-nitro-1-naphthol:
put 40 parts of 2-nitroso-1-naphthol, 150 parts of ethanol, 120 parts of water and 15 parts of caustic soda into the reaction kettle in turn, and after stirring evenly , 280 parts of aqueous hydrogen peroxide solution with a mass fraction of 30% was added dropwise, the temperature was raised to 70° C. for 35 min, and the reaction of the raw materials was followed by TLC or HPLC.
References:
CN113717052,2021,A Location in patent:Paragraph 0016-0023
90-15-3
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$9.00/5g
607-24-9
165 suppliers
$9.00/1g
581-89-5
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$55.00/250mg
607-24-9
165 suppliers
$9.00/1g