ChemicalBook CAS DataBase List 2-Octanone oxime

2-Octanone oxime synthesis

9synthesis methods

Product Name:2-Octanone oxime
CAS Number:7207-49-0
Molecular formula:C8H17NO
Molecular Weight:143.2267

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Yield:7207-49-0 87%

Reaction Conditions:

with hydroxylamine hydrochloride in pyridine at 20; for 120 h;

Steps:

3 EXAMPLE 3; Synthesis of 2-Octanone Oxime

In a 50 ml round-bottom flask, a mixture of 2-octanone, hydroxylamine hydrochloride in pyridine was stirred, at room temperature under nitrogen blanket, for five days. The reaction mixture was then concentrated under vacuum to remove most of pyridine. The oil was then dissolved in dichloromethane. The product precipitated on standing. The product was obtained as a white solid in 87% yield.

References:

US6696608,2004,B1 Location in patent:Page column 20