2-Oxaspiro[4.4]nonane, 3-(iodomethyl)- synthesis
- Product Name:2-Oxaspiro[4.4]nonane, 3-(iodomethyl)-
- CAS Number:1403649-36-4
- Molecular formula:C9H15IO
- Molecular Weight:266.12
![[1-(prop-2-en-1-yl)cyclopentyl]methanol](/CAS/20210111/GIF/441774-57-8.gif)
441774-57-8
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1403649-36-4
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Yield:1403649-36-4 94%
Reaction Conditions:
Stage #1: (1-allylcyclopentyl)methanolwith sodium hydrogencarbonate in acetonitrile at 20; for 0.5 h;Inert atmosphere;
Stage #2: with iodine in acetonitrile;Inert atmosphere;
References:
Jiao, Zhi-Wei;Zhang, Shu-Yu;He, Chuan;Tu, Yong-Qiang;Wang, Shao-Hua;Zhang, Fu-Min;Zhang, Yong-Qiang;Li, Hui [Angewandte Chemie - International Edition,2012,vol. 51,# 35,p. 8811 - 8815] Location in patent:supporting information; experimental part