2-Oxetanone, 4,4-diethyl-3-methylene- synthesis

4synthesis methods

Product Name:2-Oxetanone, 4,4-diethyl-3-methylene-
CAS Number:136066-41-6
Molecular formula:C8H12O2
Molecular Weight:140.18

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1) O₂, 2) conc.H₂SO₄ / 1) CHCl₃, tetraphenylporphine, -5 to 0 deg C, 48 h, 2) 20 deg C, 48 h
2: 9 percent / triphenylphosphine / CHCl₃ / a) -45 deg C, 15 min, b) to 20 deg C

References:

Adam, Waldemar;Albert, Rainer;Grau, Nuria Dachs;Hasemann, Ludwig;Nestler, Bernd;et al. [Journal of Organic Chemistry,1991,vol. 56,# 20,p. 5778 - 5781]

6285-06-9
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201230-82-2 Synthesis

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References

1,2-Dioxolan-3-one, 5,5-diethyl-4-methylene-

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References

96-22-0
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References