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2-Oxetanone, 4,4-diethyl-3-methylene- synthesis
- Product Name:2-Oxetanone, 4,4-diethyl-3-methylene-
- CAS Number:136066-41-6
- Molecular formula:C8H12O2
- Molecular Weight:140.18
![2-Pentenoic acid, 3-ethyl-2-methyl-](/CAS/20180601/GIF/136066-28-9.gif)
136066-28-9
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![2-Oxetanone, 4,4-diethyl-3-methylene-](/CAS/20210111/GIF/136066-41-6.gif)
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1) O2, 2) conc.H2SO4 / 1) CHCl3, tetraphenylporphine, -5 to 0 deg C, 48 h, 2) 20 deg C, 48 h
2: 9 percent / triphenylphosphine / CHCl3 / a) -45 deg C, 15 min, b) to 20 deg C
References:
Adam, Waldemar;Albert, Rainer;Grau, Nuria Dachs;Hasemann, Ludwig;Nestler, Bernd;et al. [Journal of Organic Chemistry,1991,vol. 56,# 20,p. 5778 - 5781]
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![3-Pentanone](/CAS/GIF/96-22-0.gif)
96-22-0
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$9.00/1g
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