2-(PHENYLTHIO)PYRIDINE-3-CARBONYL CHLORIDE synthesis

Yield:165249-92-3 100%

Reaction Conditions:

with oxalyl dichloride in dichloromethane;N,N-dimethyl-formamide at 20; for 0.0833333 h;Inert atmosphere;

References:

Letavic, Michael A.;Lord, Brian;Bischoff, Francois;Hawryluk, Natalie A.;Pieters, Serge;Rech, Jason C.;Sales, Zachary;Velter, Adriana I.;Ao, Hong;Bonaventure, Pascal;Contreras, Victor;Jiang, Xiaohui;Morton, Kirsten L.;Scott, Brian;Wang, Qi;Wickenden, Alan D.;Carruthers, Nicholas I.;Bhattacharya, Anindya [ACS Medicinal Chemistry Letters,2013,vol. 4,# 4,p. 419 - 422] Location in patent:supporting information