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177780-96-0

2-[(prop-2-en-1-ylamino)methyl]phenol synthesis

3synthesis methods
-

Yield:177780-96-0 95%

Reaction Conditions:

Stage #1: salicylaldehyde;1-amino-2-propenewith sodium sulfate in tetrahydrofuran at 20; for 2 h;
Stage #2: with sodium tris(acetoxy)borohydride in tetrahydrofuran; for 15 h;Further stages.;

References:

Bieraeugel, Hans;Jansen, T. Paul;Schoemaker, Hans E.;Hiemstra, Henk;Van Maarseveen, Jan H. [Organic Letters,2002,vol. 4,# 16,p. 2673 - 2674]