2-PROPANOL-1,1,1,3,3,3-D6 synthesis
- Product Name:2-PROPANOL-1,1,1,3,3,3-D6
- CAS Number:3976-29-2
- Molecular formula:C3H2D6O
- Molecular Weight:66.13
666-52-4
149 suppliers
$24.00/10g
3976-29-2
34 suppliers
$45.00/100mg
Yield:3976-29-2 100%
Reaction Conditions:
with lithium aluminium tetrahydride in diethylene glycol dimethyl ether at 0 - 20; for 1 h;
Steps:
7.1 Step 1: Example 7b
To a solution of LAH (6.3 g, 165.8 mmol) in diglyme (175 mL) was slowly added Example 7a (25.0 g, 390.6 mmol) at 0°C. After addition, the mixture was allowed to stir from 0°C to r.t. for 1 h. The reaction was quenched by adding glycol slowly at 0°C, and the resulting mixture was distilled directly (atmospheric pressure, low temperature cooling circulator) and the fraction between 79-l05°C was collected to give the desired product Example 7b (25 g, yield 100%) as colorless liquid.
References:
WO2019/240938,2019,A1 Location in patent:Paragraph 00289
666-52-4
149 suppliers
$24.00/10g
13323-81-4
103 suppliers
inquiry
3976-29-2
34 suppliers
$45.00/100mg
98-86-2
786 suppliers
$9.00/5g
666-52-4
149 suppliers
$24.00/10g
67-63-0
1599 suppliers
$18.00/25ML
3976-29-2
34 suppliers
$45.00/100mg
3972-26-7
35 suppliers
$150.00/500mg
3979-51-9
41 suppliers
$55.00/25ml