![](/CAS/GIF/3976-29-2.gif)
2-PROPANOL-1,1,1,3,3,3-D6 synthesis
- Product Name:2-PROPANOL-1,1,1,3,3,3-D6
- CAS Number:3976-29-2
- Molecular formula:C3H2D6O
- Molecular Weight:66.13
![ACETONE-D6](/CAS/GIF/666-52-4.gif)
666-52-4
134 suppliers
$24.00/10g
![2-PROPANOL-1,1,1,3,3,3-D6](/CAS/GIF/3976-29-2.gif)
3976-29-2
30 suppliers
$45.00/100mg
Yield:3976-29-2 100%
Reaction Conditions:
with lithium aluminium tetrahydride in diethylene glycol dimethyl ether at 0 - 20; for 1 h;
Steps:
7.1 Step 1: Example 7b
To a solution of LAH (6.3 g, 165.8 mmol) in diglyme (175 mL) was slowly added Example 7a (25.0 g, 390.6 mmol) at 0°C. After addition, the mixture was allowed to stir from 0°C to r.t. for 1 h. The reaction was quenched by adding glycol slowly at 0°C, and the resulting mixture was distilled directly (atmospheric pressure, low temperature cooling circulator) and the fraction between 79-l05°C was collected to give the desired product Example 7b (25 g, yield 100%) as colorless liquid.
References:
WO2019/240938,2019,A1 Location in patent:Paragraph 00289
![ACETONE-D6](/CAS/GIF/666-52-4.gif)
666-52-4
134 suppliers
$24.00/10g
![ALPHA-METHYLBENZYL ALCOHOL](/CAS/GIF/13323-81-4.gif)
13323-81-4
96 suppliers
inquiry
![2-PROPANOL-1,1,1,3,3,3-D6](/CAS/GIF/3976-29-2.gif)
3976-29-2
30 suppliers
$45.00/100mg
![Acetophenone](/CAS/GIF/98-86-2.gif)
98-86-2
743 suppliers
$9.00/5g
![ACETONE-D6](/CAS/GIF/666-52-4.gif)
666-52-4
134 suppliers
$24.00/10g
![Isopropyl alcohol](/CAS/GIF/67-63-0.gif)
67-63-0
1550 suppliers
$18.00/25ML
![2-PROPANOL-1,1,1,3,3,3-D6](/CAS/GIF/3976-29-2.gif)
3976-29-2
30 suppliers
$45.00/100mg
![2-PROPAN-2-D-OL](/CAS/GIF/3972-26-7.gif)
3972-26-7
31 suppliers
$150.00/500mg
![Isopropanol-d](/CAS/GIF/3979-51-9.gif)
3979-51-9
37 suppliers
$55.00/25ml