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2-Propenal, 2,3-dihydroxy-, (Z)- (9CI) synthesis

1synthesis methods
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Yield:52126-82-6 53%

Reaction Conditions:

Stage #1: divinylcarbinolwith oxygen;ozone in methanol at -70; for 1 h;
Stage #2: with hydrogen;palladium on activated charcoal in methanol at 0; for 1 h;Further stages.;

References:

Schank, Kurt;Buegler, Stephan;Folz, Harald;Schott, Norbert [Helvetica Chimica Acta,2007,vol. 90,# 8,p. 1606 - 1649]