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2-Propenoic acid, 2-Methoxy- synthesis

3synthesis methods
-

Yield:32821-75-3 80%

Reaction Conditions:

with n-butyllithium;potassium-t-butoxide in tetrahydrofuran;N,N,N,N,N,N-hexamethylphosphoric triamide;hexane;1.) -70 deg C, 1 h, 2.) 25 deg C, 0.5 d;

References:

Bates, Robert B.;Caldera, Sriyani [Journal of Organic Chemistry,1993,vol. 58,# 24,p. 6920 - 6921]