2-PROPENOIC ACID, 3-(3-THIENYL)-, ETHYL ESTER synthesis
- Product Name:2-PROPENOIC ACID, 3-(3-THIENYL)-, ETHYL ESTER
- CAS Number:50266-60-9
- Molecular formula:C9H10O2S
- Molecular Weight:182.24
Yield:50266-60-9 100%
Reaction Conditions:
Stage #1: diethoxyphosphoryl-acetic acid ethyl esterwith sodium hydride in tetrahydrofuran;mineral oil at 0 - 20; for 0.5 h;
Stage #2: 3-Thiophenecarboxaldehyde in tetrahydrofuran;mineral oil at 20; for 1 h;
References:
Sengmany, Stephane;Ceballos, Claire;Belhadj, Romain;Cachet-Vivier, Christine;Gall, Erwan Le;Brissault, Blandine;Penelle, Jacques;Leonel, Eric [Journal of Polymer Science, Part A: Polymer Chemistry,2012,vol. 50,# 5,p. 900 - 911] Location in patent:experimental part
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50266-60-9
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