2-(TERT-BUTOXYCARBONYLAMINO)HEX-5-ENOIC ACID synthesis

9synthesis methods

Product Name:2-(TERT-BUTOXYCARBONYLAMINO)HEX-5-ENOIC ACID
CAS Number:214206-61-8
Molecular formula:C11H19NO4
Molecular Weight:229.27

24424-99-5 Synthesis

24424-99-5
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1237001-51-2
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2-(TERT-BUTOXYCARBONYLAMINO)HEX-5-ENOIC ACID

214206-61-8
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Yield:214206-61-8 94%

Reaction Conditions:

Stage #1: di-tert-butyl dicarbonate;2-amino-hex-5-enoic acid hydrochloridewith N-ethyl-N,N-diisopropylamine in 1,4-dioxane;water at 20;Inert atmosphere;
Stage #2: with hydrogenchloride in diethyl ether;water;

References:

Plé, Karen;Haudrechy, Arnaud;Probst, Nicolas P. [Tetrahedron,2010,vol. 66,# 27-28,p. 5030 - 5035] Location in patent:experimental part

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756498-97-2
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214206-61-8
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References

(2S)-BOC-2-AMINO-5-HEXENOIC ACID METHYL ESTER

92136-57-7
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References

5-Hexenoic acid, 2-[(diphenylmethylene)amino]-, ethyl ester

912651-56-0
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214206-61-8
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References

24424-99-5 Synthesis

24424-99-5
823 suppliers
$13.50/25G

214206-61-8
30 suppliers
inquiry

References