2-TERT-BUTYL-6-METHYLPHENYL ISOCYANATE synthesis
- Product Name:2-TERT-BUTYL-6-METHYLPHENYL ISOCYANATE
- CAS Number:13680-30-3
- Molecular formula:C12H15NO
- Molecular Weight:189.25
32315-10-9
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Yield:-
Reaction Conditions:
Stage #1: bis(trichloromethyl) carbonatewith triethylamine in dichloromethane at 0; for 0.0833333 h;
Stage #2: 2-tert-butyl-6-methylaniline in dichloromethane at 20;
References:
Jin, Jiamiao;Huang, Xuan;Xu, Jun;Li, Tingting;Peng, Xiaolin;Zhu, Xun;Zhang, Junmin;Jin, Zhichao;Chi, Yonggui Robin [Organic Letters,2021,vol. 23,# 10,p. 3991 - 3996] Location in patent:supporting information