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2-Thiocyanato-2-methylpropane synthesis

12synthesis methods
-

Yield:37985-18-5 73%

Reaction Conditions:

Stage #1: zinc(II) thiocyanatewith titanium tetrachloride in dichloromethane; for 0.166667 h;ultrasound irradiation;
Stage #2: tertiary butyl chloridewith pyridine in dichloromethane at 25; for 5 h;ultrasound irradiation;

References:

Bettadaiah;Gurudutt;Srinivas [Synthetic Communications,2003,vol. 33,# 13,p. 2293 - 2299]