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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

2-Thiopheneacetonitrile, α-(phenylsulfonyl)- synthesis

1synthesis methods
1003-09-4 Synthesis
2-Bromothiophene

1003-09-4
470 suppliers
$10.00/25g

7605-28-9 Synthesis
(PHENYLSULFONYL)ACETONITRILE

7605-28-9
144 suppliers
$7.00/1g

2-Thiopheneacetonitrile, α-(phenylsulfonyl)-

130138-43-1
3 suppliers
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Yield:130138-43-1 84%

Reaction Conditions:

with sodium hydride;tetrakis(triphenylphosphine) palladium(0) in 1,2-dimethoxyethane; for 2 h;Heating;

References:

Sakamoto;Katoh;Kondo;Yamanaka [Chemical and Pharmaceutical Bulletin,1990,vol. 38,# 6,p. 1513 - 1517]