2-(trifluoromethyl)-1,4-Benzenedicarboxylic acid synthesis
- Product Name:2-(trifluoromethyl)-1,4-Benzenedicarboxylic acid
- CAS Number:1483-47-2
- Molecular formula:C9H5F3O4
- Molecular Weight:234.13
553-94-6
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: magnesium / tetrahydrofuran / Inert atmosphere; Reflux
1.2: -78 - 20 °C / Inert atmosphere
1.3: Reflux
2.1: copper(l) chloride; tert.-butylhydroperoxide / dichloromethane; methanol; water / 12 h / 0 - 20 °C
3.1: nitric acid / water / 24 h / 180 °C
References:
Horcajada, Patricia;Chevreau, Hubert;Heurtaux, Daniela;Benyettou, Farah;Salles, Fabrice;Devic, Thomas;Garcia-Marquez, Alfonso;Yu, Cihang;Lavrard, Hubert;Dutson, Claire L.;Magnier, Emmanuel;Maurin, Guillaume;Elkaïm, Erik;Serre, Christian [Chemical Communications,2014,vol. 50,# 52,p. 6872 - 6874]
84796-70-3
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1483-47-2
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120985-64-0
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$29.00/100mg
1483-47-2
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1000210-73-0
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1483-47-2
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