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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

tert-butyl [6-(hydroxymethyl)pyridin-2-yl]carbamate synthesis

12synthesis methods
2-Pyridinecarboxylic acid, 6-[bis[(1,1-dimethylethoxy)carbonyl]amino]-, ethyl ester

1219130-09-2
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tert-butyl [6-(hydroxymethyl)pyridin-2-yl]carbamate

203321-83-9
38 suppliers
$45.00/25mg

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Yield:203321-83-9 99%

Reaction Conditions:

with sodium tetrahydroborate;calcium chloride in ethanol at 0 - 20; for 3.33333 h;

References:

Majgier-Baranowska, Helena;Li, Bing;Peet, Norton P. [Synthetic Communications,2013,vol. 43,# 8,p. 1173 - 1180]

Ethyl 6-((tert-butoxycarbonyl)aMino)picolinate

203321-86-2
20 suppliers
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tert-butyl [6-(hydroxymethyl)pyridin-2-yl]carbamate

203321-83-9
38 suppliers
$45.00/25mg

References
6-[[(1,1-DIMETHYLETHOXY)CARBONYL]AMINO]-2PYRIDINECARBOXYLIC ACID METHYL ESTER

258497-48-2
31 suppliers
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tert-butyl [6-(hydroxymethyl)pyridin-2-yl]carbamate

203321-83-9
38 suppliers
$45.00/25mg

References
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
821 suppliers
$13.50/25G

tert-butyl [6-(hydroxymethyl)pyridin-2-yl]carbamate

203321-83-9
38 suppliers
$45.00/25mg

References
69142-64-9 Synthesis
6-Aminopyridine-2-carboxylic acid ethyl ester

69142-64-9
88 suppliers
$8.00/100mg

tert-butyl [6-(hydroxymethyl)pyridin-2-yl]carbamate

203321-83-9
38 suppliers
$45.00/25mg

References