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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

2-(Chloromethyl)-1-methyl-5-nitro-1H-1,3-benzodiazole synthesis

3synthesis methods
Chloroacetic acid

79-11-8
10 suppliers
$27.00/25g

41939-61-1 Synthesis
N1-Methyl-4-nitro-o-phenyldiamin

41939-61-1
189 suppliers
$9.00/1g

2-(Chloromethyl)-1-methyl-5-nitro-1H-1,3-benzodiazole

20443-39-4
9 suppliers
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Yield:20443-39-4 71%

Reaction Conditions:

with hydrogenchloride in water; for 4 h;Reflux;

References:

Bai, Yu-Bin;Zhang, An-Ling;Tang, Jiang-Jiang;Gao, Jin-Ming [Journal of Agricultural and Food Chemistry,2013,vol. 61,# 11,p. 2789 - 2795]