6-Chloro-9-(2,3,5-tri-O-benzoyl-2-C-methyl-beta-D-ribofuranosyl)-9H-purine synthesis
- Product Name:6-Chloro-9-(2,3,5-tri-O-benzoyl-2-C-methyl-beta-D-ribofuranosyl)-9H-purine
- CAS Number:205171-04-6
- Molecular formula:C32H25ClN4O7
- Molecular Weight:613.02
98-88-4
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205171-04-6
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: pyridine / neat (no solvent) / 16 h / 20 °C
2: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 4 h / 20 °C
3: pyridine / neat (no solvent) / 4 h / 60 °C
4: 1,8-diazabicyclo[5.4.0]undec-7-ene; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 5.25 h / 0 - 65 °C
References:
WO2018/31818,2018,A2
87-42-3
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15397-15-6
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205171-04-6
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7392-74-7
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205171-04-6
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22224-41-5
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205171-04-6
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157037-56-4
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205171-04-6
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