![](/StructureFile/ChemBookStructure4/GIF/CB4136790.gif)
AMINO([2-(METHOXYCARBONYL)BENZYL]SULFANYL)METHANIMINIUM BROMIDE synthesis
- Product Name:AMINO([2-(METHOXYCARBONYL)BENZYL]SULFANYL)METHANIMINIUM BROMIDE
- CAS Number:21784-51-0
- Molecular formula:C10H13BrN2O2S
- Molecular Weight:305.19
Yield:21784-51-0 100%
Reaction Conditions:
in methanol; for 4 h;Heating / reflux;
Steps:
13.2
A mixture of the crude bromide from Step 1 (7.2 g, 0.031 mmol) and thiourea (2.6 g, 35 mmol) in MeOH (40 mL) was heated to reflux for 4 h, cooled to room temperature, and concentrated to afford methyl 2-({[amino(imino)methyl]thio}methyl)benzoate hydrobromide (10 g, ca. 100%), which was used without purification.
References:
WO2006/128142,2006,A2 Location in patent:Page/Page column 41
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89-71-4
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21784-51-0
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