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1,3-Methanonaphthalen-5(1H)-one, 2,3,4,6,7,8-hexahydro-2,2-dimethyl- synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 84 percent / hydroquinone / 48 h / 70 - 72 °C / Pyrex tube
2: 55 percent / tri-n-butylamine / 48 h / 150 - 152 °C

References:

Moore, Lionel;Gooding, David;Wolinsky, Joseph [Journal of Organic Chemistry,1983,vol. 48,# 21,p. 3750 - 3754]