3-[2-(2,5-dimethylthiophen-3-yl)cyclopenten-1-yl]-2,5-dimethylthiophene synthesis

2synthesis methods

Product Name:3-[2-(2,5-dimethylthiophen-3-yl)cyclopenten-1-yl]-2,5-dimethylthiophene
CAS Number:219537-98-1
Molecular formula:C17H20S2
Molecular Weight:288.47

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3-[2-(2,5-dimethylthiophen-3-yl)cyclopenten-1-yl]-2,5-dimethylthiophene

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 54 percent / AlCl₃ / CS₂ / 2 h / Heating
2: 58 percent / Mg; TiCl₃*3THF / tetrahydrofuran / 2 h / 40 °C

References:

Lucas, Linda N.;De Jong, Jaap J. D.;Van Esch, Jan H.;Kellogg, Richard M.;Feringa, Ben L. [European Journal of Organic Chemistry,2003,# 1,p. 155 - 166]

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References