Ethanamine, 2-[[2-(ethylthio)ethyl]thio]-N-[2-[[2-(ethylthio)ethyl]thio]ethyl]- synthesis
- Product Name:Ethanamine, 2-[[2-(ethylthio)ethyl]thio]-N-[2-[[2-(ethylthio)ethyl]thio]ethyl]-
- CAS Number:219658-99-8
- Molecular formula:C12H27NS4
- Molecular Weight:313.61
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Yield:219658-99-8 89%
Reaction Conditions:
Stage #1: 2-ethylsulfanyl-ethanethiolwith sodium in ethanol;Reflux;Inert atmosphere;
Stage #2: bis-(2-chloroethyl)amine hydrochloride in ethanol; for 4 h;Reflux;Inert atmosphere;
References:
Liu, Wei;Dong, Hui;Zhang, Limin;Tian, Yang [Angewandte Chemie - International Edition,2017,vol. 56,# 51,p. 16328 - 16332][Angew. Chem.,2017,vol. 129,# 51,p. 16546 - 16550,5] Location in patent:supporting information
