(3-BroMo-2,6-diMethoxy-4-pyridyl)diphenylphosphine oxide synthesis
- Product Name:(3-BroMo-2,6-diMethoxy-4-pyridyl)diphenylphosphine oxide
- CAS Number:220998-36-7
- Molecular formula:C19H17BrNO3P
- Molecular Weight:418.22
13445-16-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: lithium diisopropylamide / tetrahydrofuran / 0.33 h / -78 °C
1.2: 90 percent / tetrahydrofuran / -78 - 20 °C
2.1: 99 percent / aq. H2O2 / acetone / 0 °C
References:
Wu, Jing;Au-Yeung, Terry T.-L.;Kwok, Wai-Him;Ji, Jian-Xin;Zhou, Zhongyuan;Yeung, Chi-Hung;Chan, Albert S. C. [Advanced Synthesis and Catalysis,2005,vol. 347,# 4,p. 507 - 511]
6231-18-1
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