Pentanoic acid, 5,5,5-trifluoro-4-oxo-, methyl ester synthesis

1synthesis methods

Product Name:Pentanoic acid, 5,5,5-trifluoro-4-oxo-, methyl ester
CAS Number:22581-31-3
Molecular formula:C6H7F3O3
Molecular Weight:184.11

Butanedioic acid, 2-(2,2,2-trifluoroacetyl)-, 1,4-dimethyl ester

244300-80-9
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Pentanoic acid, 5,5,5-trifluoro-4-oxo-, methyl ester

22581-31-3
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Yield:-

Reaction Conditions:

with boric acid at 150 - 180; for 3 h;Inert atmosphere;

References:

Wan, Wen;Hou, Jie;Jiang, Haizhen;Wang, Yangli;Zhu, Shizheng;Deng, Hongmei;Hao, Jian [Tetrahedron,2009,vol. 65,# 21,p. 4212 - 4219] Location in patent:experimental part