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ChemicalBook CAS DataBase List 3-NAPHTHALEN-1-YL-3-OXO-PROPIONIC ACID METHYL ESTER

3-NAPHTHALEN-1-YL-3-OXO-PROPIONIC ACID METHYL ESTER synthesis

3synthesis methods
-

Yield:226931-47-1 92%

Reaction Conditions:

Stage #1: carbonic acid dimethyl esterwith sodium hydride at 20;Inert atmosphere;
Stage #2: 1'-naphthacetophenone for 4 h;Inert atmosphere;Reflux;

References:

Balamurugan, Rengarajan;Manojveer, Seetharaman [Chemical Communications,2011,vol. 47,# 39,p. 11143 - 11145] Location in patent:supporting information; experimental part