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ChemicalBook CAS DataBase List Nickel, (2,2'-bipyridine-κN1,κN1')dichloro-, (SP-4-2)-

Nickel, (2,2'-bipyridine-κN1,κN1')dichloro-, (SP-4-2)- synthesis

8synthesis methods
-

Yield:12130-66-4 53%

Reaction Conditions:

in tetrahydrofuran;Pt and org. compds. suspended in THF, cooled to -10°C, added soln. of Ni compd. dropwise; warmed to room temp., filtered, vol. of filtrate reduced, cooled to -18°C, after 24 h isolated, dissolved in toluene, filtered, solvent evapd., filtered, dried in vac.;

References:

Walther, Dirk;Heubach, Kirstin;Boettcher, Lars;Schreer, Heike;Goerls, Helmar [Zeitschrift fur Anorganische und Allgemeine Chemie,2002,vol. 628,# 1,p. 20 - 30]