Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

Phosphinous amide, N,N-bis(1-methylethyl)-P,P-diphenyl- synthesis

5synthesis methods
131173-04-1 Synthesis
N,N-Diisopropyl-P,P-diphenylphosphinicamide

131173-04-1
7 suppliers
$22.60/1g

Phosphinous amide, N,N-bis(1-methylethyl)-P,P-diphenyl-

22859-57-0
2 suppliers
inquiry

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: oxalyl dichloride / dichloromethane / 1 h / 20 °C / Schlenk technique; Inert atmosphere; Sealed tube
2: hexachlorodisilane / dichloromethane-d2 / 0.08 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

References:

Kapuśniak, Łukasz;Plessow, Philipp N.;Trzybiński, Damian;Woźniak, Krzysztof;Hofmann, Peter;Jolly, Phillip Iain [Organometallics,2021,vol. 40,# 6,p. 693 - 701]