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N,N-Dimethyl-1-(1H-pyrrolo[3,2-b]pyridin-3-yl)methanamine synthesis

1synthesis methods
-

Yield:23612-34-2 99%

Reaction Conditions:

in butan-1-ol; for 3 h;Reflux;

References:

Shultz, Michael D.;Cao, Xueying;Chen, Christine H.;Cho, Young Shin;Davis, Nicole R.;Eckman, Joe;Fan, Jianmei;Fekete, Alex;Firestone, Brant;Flynn, Julie;Green, Jack;Growney, Joseph D.;Holmqvist, Mats;Hsu, Meier;Jansson, Daniel;Jiang, Lei;Kwon, Paul;Liu, Gang;Lombardo, Franco;Lu, Qiang;Majumdar, Dyuti;Meta, Christopher;Perez, Lawrence;Pu, Minying;Ramsey, Tim;Remiszewski, Stacy;Skolnik, Suzanne;Traebert, Martin;Urban, Laszlo;Uttamsingh, Vinita;Wang, Ping;Whitebread, Steven;Whitehead, Lewis;Yan-Neale, Yan;Yao, Yung-Mae;Zhou, Liping;Atadja, Peter [Journal of Medicinal Chemistry,2011,vol. 54,# 13,p. 4752 - 4772] Location in patent:experimental part