ChemicalBook CAS DataBase List Hydrazine, [[4-(phenylmethoxy)phenyl]methyl]-, hydrochloride

Hydrazine, [[4-(phenylmethoxy)phenyl]methyl]-, hydrochloride synthesis

1synthesis methods

Product Name:Hydrazine, [[4-(phenylmethoxy)phenyl]methyl]-, hydrochloride
CAS Number:237064-54-9
Molecular formula:C14H17ClN2O
Molecular Weight:264.75

836-42-0
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Hydrazine, [[4-(phenylmethoxy)phenyl]methyl]-, hydrochloride

237064-54-9
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Yield:237064-54-9 72%

Reaction Conditions:

Stage #1: 4-benzyloxybenzyl chloridewith hydrazine hydrate in 1,4-dioxane;ethanol; for 10 h;Reflux;
Stage #2: with hydrogenchloride in water;

References:

Murakawa, Takeshi;Hayashi, Hideyuki;Taki, Masayasu;Yamamoto, Yukio;Kawano, Yoshiaki;Tanizawa, Katsuyuki;Okajima, Toshihide [Journal of Biochemistry,2012,vol. 151,# 2,p. 167 - 178] Location in patent:experimental part