(16α)-17-Hydroxy-16-methyl-21-[(methylsulfonyl)oxy]pregna-1,4,9(11)-triene-3,20-dione synthesis
1synthesis methods
- Product Name:(16α)-17-Hydroxy-16-methyl-21-[(methylsulfonyl)oxy]pregna-1,4,9(11)-triene-3,20-dione
- CAS Number:23776-75-2
- Molecular formula:C23H30O6S
- Molecular Weight:434.55
Yield:23776-75-2 85%
Reaction Conditions:
with pyridine at 0 - 2; for 1.5 h;
References:
Shapiro;Gentles;Tiberi;Popper;Berkenkopf;Lutsky;Watnick [Journal of Medicinal Chemistry,1987,vol. 30,# 6,p. 1068 - 1073]