α-Phenyl-N-(phenylmethyl)benzenemethanamine Hydrochloride synthesis
1synthesis methods
- Product Name:α-Phenyl-N-(phenylmethyl)benzenemethanamine Hydrochloride
- CAS Number:23934-60-3
- Molecular formula:C20H20ClN
- Molecular Weight:309.84
Yield:23934-60-3 71%
Reaction Conditions:
Stage #1: benzophenone;benzonitrilewith hydrogen in 2-methyltetrahydrofuran at 110; under 11251.1 Torr; for 20 h;High pressure;Autoclave;
Stage #2: with hydrogenchloride in diethyl ether;
References:
Sch?nauer, Timon;Thom?, Sabrina L. J.;Kaiser, Leah;Zobel, Mirijam;Kempe, Rhett [Chemistry - A European Journal,2021,vol. 27,# 5,p. 1609 - 1614] Location in patent:supporting information