1-(3,4-METHYLENEDIOXY-PHENYL)-4,4-DIMETHYL-PENT-1-EN-3-ONE synthesis
- Product Name:1-(3,4-METHYLENEDIOXY-PHENYL)-4,4-DIMETHYL-PENT-1-EN-3-ONE
- CAS Number:2419-68-3
- Molecular formula:C14H16O3
- Molecular Weight:232.27
75-97-8
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120-57-0
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2419-68-3
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$141.19/100mg
Yield: 88%
Reaction Conditions:
with sodium hydroxide in ethanol at 40; for 1 h;
Steps:
1.1
2 g NaOH solid was dissolved in 100mL ethanol, 0.1 mol of piperonal and 0.13 mol of pinacolone were added, and reacted at 40°C for 1 h. Some of the solvent was removed by steaming, frozen, filtered and dried to obtain pale yellow solid 2,2-dimethyl5-(3,4-methylenedioxy)-4-ene-3-pentanone,Yield 88%.
References:
HUNAN UNIVERSITY;HU, AIXI;WU, ZHILIN;YE, JIAO;DING, NA CN104530035, 2016, B Location in patent:Paragraph 0024; 0026
49763-96-4
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$6.00/5mg
2419-68-3
31 suppliers
$141.19/100mg
274-09-9
456 suppliers
$5.00/5g
2419-68-3
31 suppliers
$141.19/100mg