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1,2-Ethanediamine, N1,N2-diethyl-N1,N2-bis[2-(ethylamino)ethyl]- synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 65 percent / acetic acid / 10 h / Ambient temperature
2: 77 percent / LiAlH4 / tetrahydrofuran / 48 h / Heating

References:

Krakowiak, Krzysztof E.;Bradshaw, Jerald S.;Forsnes, Evan V.;Izatt, Reed M. [Journal of Heterocyclic Chemistry,1989,vol. 26,p. 661 - 665]