ChemicalBook CAS DataBase List DIETHYL (4-{BIS-[4-(DIETHOXY-PHOSPHORYLMETHYL)-PHENYL]-AMINO}-BENZYL)-PHOSPHONATE

DIETHYL (4-{BIS-[4-(DIETHOXY-PHOSPHORYLMETHYL)-PHENYL]-AMINO}-BENZYL)-PHOSPHONATE synthesis

3synthesis methods

Product Name:DIETHYL (4-{BIS-[4-(DIETHOXY-PHOSPHORYLMETHYL)-PHENYL]-AMINO}-BENZYL)-PHOSPHONATE
CAS Number:245653-28-5
Molecular formula:C33H48NO9P3
Molecular Weight:695.66

119001-43-3
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DIETHYL (4-{BIS-[4-(DIETHOXY-PHOSPHORYLMETHYL)-PHENYL]-AMINO}-BENZYL)-PHOSPHONATE

245653-28-5
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 92 percent / KBH₄ / ethanol; CH₂Cl₂ / 5 h / 20 °C
2: 85 percent / HBr / H₂O / 5 h / Heating
3: 59 percent / 72 h / Heating

References:

Mongin, Olivier;Porrès, Laurent;Katan, Claudine;Pons, Thomas;Mertz, Jerome;Blanchard-Desce, Mireille [Tetrahedron Letters,2003,vol. 44,# 44,p. 8121 - 8125]

263242-49-5
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245653-28-5
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References

603-34-9
313 suppliers
$24.89/5g

245653-28-5
7 suppliers
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References