![](/StructureFile/ChemBookStructure4/GIF/CB3235083.gif)
2-(4-CARBOXYBUTYRYL)AMINO-5-METHYL-1,3,4-THIADIAZOLE synthesis
1synthesis methods
- Product Name:2-(4-CARBOXYBUTYRYL)AMINO-5-METHYL-1,3,4-THIADIAZOLE
- CAS Number:247225-30-5
- Molecular formula:C8H11N3O3S
- Molecular Weight:229.26
Yield:-
Reaction Conditions:
Stage #1: glutaric anhydride,;1-(1-ethoxyethylidene)thiosemicarbazide in methanol; for 0.416667 h;Reflux;
Stage #2: with aminosulfonic acid in methanol; for 1 h;Reflux;
References:
Toche;Janrao;Gangurde;Nikam [Synthetic Communications,2013,vol. 43,# 18,p. 2527 - 2535] Location in patent:supporting information