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METHYL 2-([(4-METHOXYPHENYL)SULFONYL]AMINO)-2-PHENYLACETATE synthesis

2synthesis methods
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Yield:251096-82-9 40 %Spectr. ,119059-70-0 20 %Spectr. ,31401-17-9 22 %Spectr.

Reaction Conditions:

Stage #1: carbon dioxide;4-methoxybenzene sulfonamide;benzaldehydewith trimethylsilyltributyltin;cesium fluoride in N,N-dimethyl-formamide at 100; under 7500.75 Torr; for 3 h;Autoclave;
Stage #2: diazomethyl-trimethyl-silane in methanol;diethyl ether;

References:

Mita, Tsuyoshi;Higuchi, Yuki;Sato, Yoshihiro [Chemistry - A European Journal,2013,vol. 19,# 3,p. 1123 - 1128]