ChemicalBook CAS DataBase List N-[(S)-5,6,7,9-Tetrahydro-1,2,3,10-tetramethoxy-9-oxobenzo[a]heptalen-7-yl]-2,2,2-trifluoroacetamide

N-[(S)-5,6,7,9-Tetrahydro-1,2,3,10-tetramethoxy-9-oxobenzo[a]heptalen-7-yl]-2,2,2-trifluoroacetamide synthesis

6synthesis methods

Product Name:N-[(S)-5,6,7,9-Tetrahydro-1,2,3,10-tetramethoxy-9-oxobenzo[a]heptalen-7-yl]-2,2,2-trifluoroacetamide
CAS Number:26195-65-3
Molecular formula:C22H22F3NO6
Molecular Weight:453.41

68296-64-0 Synthesis

68296-64-0
8 suppliers
inquiry

N-[(S)-5,6,7,9-Tetrahydro-1,2,3,10-tetramethoxy-9-oxobenzo[a]heptalen-7-yl]-2,2,2-trifluoroacetamide

26195-65-3
14 suppliers
$716.10/50MG

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 79 percent / Na₂CO₃ / diethyl ether / 2.5 h / Ambient temperature
2: 46 percent / methanol; diethyl ether / 3 h
3: 70 percent / K₂CO₃ / acetone; H₂O / 60 °C
5: 75 percent / Na₂CO₃ / diethyl ether / 2.5 h / Ambient temperature

References:

Dumont;Brossi;Silverton [Journal of Organic Chemistry,1986,vol. 51,# 13,p. 2515 - 2521]