α-(p-Tolylsulfonyl)-a-(thien-3-yl)methyl)isocyanide synthesis
- Product Name:α-(p-Tolylsulfonyl)-a-(thien-3-yl)methyl)isocyanide
- CAS Number:263389-44-2
- Molecular formula:C13H11NO2S2
- Molecular Weight:277.3619
![Formamide, N-[[(4-methylphenyl)sulfonyl]-3-thienylmethyl]-](/CAS/20180529/GIF/185243-98-5.gif)
185243-98-5
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263389-44-2
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Yield:263389-44-2 76%
Reaction Conditions:
Stage #1: N-(thiophen-3-yl(tosyl)methyl)formamidewith trichlorophosphate in tetrahydrofuran at 25; for 0.0833333 h;
Stage #2: with triethylamine in tetrahydrofuran at 0 - 10;
References:
Sisko, Joseph;Mellinger, Mark;Sheldrake, Peter W.;Baine, Neil H.;Dong, Yan;Wolff, Steven [Organic Syntheses,2000,vol. 77,p. 198 - 198]
536-57-2
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$34.00/1g
263389-44-2
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498-62-4
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$5.00/1g
263389-44-2
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824-79-3
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$6.00/25g
263389-44-2
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