ChemicalBook CAS DataBase List (2-methoxy-3,6-dioxabicyclo[3.1.0]hex-4-yl)methanol

(2-methoxy-3,6-dioxabicyclo[3.1.0]hex-4-yl)methanol synthesis

6synthesis methods

Product Name:(2-methoxy-3,6-dioxabicyclo[3.1.0]hex-4-yl)methanol
CAS Number:26532-10-5
Molecular formula:C6H10O4
Molecular Weight:146.14

α-D-Xylofuranoside, methyl 3,5-O-(1-methylethylidene)-, 2-(4-methylbenzenesulfonate)

551929-55-6
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(2-methoxy-3,6-dioxabicyclo[3.1.0]hex-4-yl)methanol

26532-10-5
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Yield:26532-10-5 92%

Reaction Conditions:

Stage #1: methyl-[O³,O⁵-isopropylidene-O²-(toluene-4-sulfonyl)-α-D-xylofuranoside]with acetic acid at 50; for 2 h;
Stage #2: with sodium methylate in methanol at 0 - 10;

References:

Lim, Moo Hong;Kim, Hea Ok;Moon, Hyung Ryong;Lee, Seung Jin;Chun, Moon Woo;Gao, Zhan-Guo;Melman, Neli;Jacobson, Kenneth A.;Kim, Joong Hyup;Jeong, Lak Shin [Bioorganic and Medicinal Chemistry Letters,2003,vol. 13,# 5,p. 817 - 820]

56607-40-0
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$60.00/1g

26532-10-5
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References

79083-42-4
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43168-73-6
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26532-10-5
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References

METHYL-3,5-O-ISOPROPYLIDENE-ALPHA-D-XYLOFURANOSIDE

7045-40-1
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26532-10-5
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References

1824-96-0
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26532-10-5
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References