ChemicalBook CAS DataBase List N-{3-[(2,6-DiMethylphenyl)aMino]-1-Methyl-2-buten-1-ylidene}-2,6-diMethylbenzenaMine, 98%

N-{3-[(2,6-DiMethylphenyl)aMino]-1-Methyl-2-buten-1-ylidene}-2,6-diMethylbenzenaMine, 98% synthesis

1synthesis methods

Product Name:N-{3-[(2,6-DiMethylphenyl)aMino]-1-Methyl-2-buten-1-ylidene}-2,6-diMethylbenzenaMine, 98%
CAS Number:267431-79-8
Molecular formula:C21H26N2
Molecular Weight:306.44

87-62-7
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$10.00/5G

123-54-6 Synthesis

123-54-6
570 suppliers
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N-{3-[(2,6-DiMethylphenyl)aMino]-1-Methyl-2-buten-1-ylidene}-2,6-diMethylbenzenaMine, 98%

267431-79-8
26 suppliers
$74.00/250mg

Yield:267431-79-8 85%

Reaction Conditions:

Stage #1: 2,6-dimethylaniline;acetylacetonewith hydrogenchloride in water at 85; for 0.5 h;Microwave irradiation;Inert atmosphere;
Stage #2: with sodium carbonate in water at 20;Inert atmosphere;

References:

Lee, Dong-Hwan;Jung, Ji-Young;Jin, Myung-Jong [Chemical Communications,2010,vol. 46,# 47,p. 9046 - 9048] Location in patent:supporting information; experimental part