ChemicalBook CAS DataBase List 1-Pyrrolidinyloxy, 3-(hydroxymethyl)-2,2,5,5-tetramethyl-

1-Pyrrolidinyloxy, 3-(hydroxymethyl)-2,2,5,5-tetramethyl- synthesis

1synthesis methods

Product Name:1-Pyrrolidinyloxy, 3-(hydroxymethyl)-2,2,5,5-tetramethyl-
CAS Number:27298-75-5
Molecular formula:C9H18NO2
Molecular Weight:0

3-Carboxy-2,2,5,5-tetraMethylpyrrolidine 1-Oxyl Free Radical

2154-68-9
73 suppliers
$25.52/50mg

1-Pyrrolidinyloxy, 3-(hydroxymethyl)-2,2,5,5-tetramethyl-

27298-75-5
12 suppliers
$515.00/50mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1: triethylamine / tetrahydrofuran / 1 h / Ambient temperature
2: lithium aluminum hydride / tetrahydrofuran / 0 deg C, 30 min, then water, rt, overnight

References:

Renk, Geoffrey E.;Or, Yat Sun;Crouch, Rosalie K. [Journal of the American Chemical Society,1987,vol. 109,# 20,p. 6163 - 6168]