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ChemicalBook CAS DataBase List 1,2,3,3a,4,8b-hexahydro-4-(4-Methylpheny)-Cyclopent[b]indole
273220-33-0

1,2,3,3a,4,8b-hexahydro-4-(4-Methylpheny)-Cyclopent[b]indole synthesis

2synthesis methods
80278-94-0 Synthesis
1,2,3,3A,4,8B-HEXAHYDROCYCLOPENTA[B]INDOLE

80278-94-0
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1,2,3,3a,4,8b-hexahydro-4-(4-Methylpheny)-Cyclopent[b]indole

273220-33-0
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Yield:273220-33-0 91%

Reaction Conditions:

with palladium diacetate;sodium t-butanolate;tris[tert-butyl]phosphonium tetrafluoroborate in toluene at 95; for 9 h;Inert atmosphere;Buchwald-Hartwig Coupling;

References:

Song, Heli;Zhang, Jing;Jin, Jiamin;Wang, Haifeng;Xie, Yongshu [Journal of Materials Chemistry C,2018,vol. 6,# 15,p. 3927 - 3936]