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ChemicalBook CAS DataBase List BIPY531, 2,2'-([2,2'-Bipyridine]-5,5'-diyl)diacetonitrile
286380-59-4

BIPY531, 2,2'-([2,2'-Bipyridine]-5,5'-diyl)diacetonitrile synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 50.6 percent / N-chlorosuccinimide; benzoyl peroxide / CCl4 / 48 h / Heating
2: 59.3 percent / conc. hydrochloric acid / ethanol; H2O / 2.5 h / Heating

References:

Lindner, Ekkehard;Veigel, Robert;Ortner, Kirstin;Nachtigal, Christiane;Steimann, Manfred [European Journal of Inorganic Chemistry,2000,# 5,p. 959 - 969]