![](/CAS/20150408/GIF/286936-08-1.gif)
(2S,3S,4aR,8R,8aR)-Hexahydro-8-hydroxy-2,3-diMethoxy-2,3-diMethyl-1,4-benzodioxin-6(5H)-one synthesis
- Product Name:(2S,3S,4aR,8R,8aR)-Hexahydro-8-hydroxy-2,3-diMethoxy-2,3-diMethyl-1,4-benzodioxin-6(5H)-one
- CAS Number:286936-08-1
- Molecular formula:C12H20O6
- Molecular Weight:260.28
![Quinic acid](/CAS/GIF/77-95-2.gif)
77-95-2
285 suppliers
$19.80/5G
![(2S,3S,4aR,8R,8aR)-Hexahydro-8-hydroxy-2,3-diMethoxy-2,3-diMethyl-1,4-benzodioxin-6(5H)-one](/CAS/20150408/GIF/286936-08-1.gif)
286936-08-1
6 suppliers
$165.00/50mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 98 percent / camphoricsulfonic acid / methanol / 12 h / Heating
2: NaBH4 / methanol / 24 h / 0 - 20 °C
3: NaIO4/SiO2 / CH2Cl2 / 1.5 h
References:
Arthurs, Claire L.;Wind, Natasha S.;Whitehead, Roger C.;Stratford, Ian J. [Bioorganic and Medicinal Chemistry Letters,2007,vol. 17,# 2,p. 553 - 557]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![(2S,3S,4aR,8R,8aR)-Hexahydro-8-hydroxy-2,3-diMethoxy-2,3-diMethyl-1,4-benzodioxin-6(5H)-one](/CAS/20150408/GIF/286936-08-1.gif)
286936-08-1
6 suppliers
$165.00/50mg
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![(2S,3S,4aR,8R,8aR)-Hexahydro-8-hydroxy-2,3-diMethoxy-2,3-diMethyl-1,4-benzodioxin-6(5H)-one](/CAS/20150408/GIF/286936-08-1.gif)
286936-08-1
6 suppliers
$165.00/50mg
![Quinic acid](/CAS/GIF/77-95-2.gif)
77-95-2
285 suppliers
$19.80/5G
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431-03-8
366 suppliers
$21.00/25mL
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149-73-5
521 suppliers
$12.00/5g
![(2S,3S,4aR,8R,8aR)-Hexahydro-8-hydroxy-2,3-diMethoxy-2,3-diMethyl-1,4-benzodioxin-6(5H)-one](/CAS/20150408/GIF/286936-08-1.gif)
286936-08-1
6 suppliers
$165.00/50mg